| TMP(g) | 二水合氯化铜(g) | 盐酸羟胺(g) | 收率% |
| 3 | 0.76 | 0.78 | 83.43 |
| 3 | 0.50 | 0.78 | 78.22 |
| 3 | 0.76 | 0.50 | 78.89 |
| 3 | 0.76 | 0.76 | 83.83 |
| 3 | 1.00 | 0.78 | 83.03 |
| 3 | 1.00 | 1.00 | 83.01 |
| 3 | 1.50 | 1.50 | 83.03 |